Separation and identification of phenol-formaldehyde condensates by gas chromatography-mass spectrometry II. Base-catalysed condensation products

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Abstract

The characterization of phenol-formaldehyde condensates obtained by base catalysis is described. Trimethylsilyl derivatives of the components were prepared and analysed by gas chromatography-mass spectrometry. Electron impact ionization mass spectra of methylolated dihydroxydiphenylmethane positional isomers are discussed. Prominent differences in ion abundances facilitate the identification of the compounds. Substituted trinuclear phenols among the reaction products are also described.

Original languageEnglish
Pages (from-to)91-98
Number of pages8
JournalJournal of Chromatography A
Volume331
Issue numberC
DOIs
StatePublished - 1 Jan 1985

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Impact ionization
Phenols
Phenol
Catalysis
Reaction products
Isomers
Gas chromatography
Gas Chromatography-Mass Spectrometry
Formaldehyde
Mass spectrometry
Condensation
Electrons
Ions
Derivatives

Cite this

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title = "Separation and identification of phenol-formaldehyde condensates by gas chromatography-mass spectrometry II. Base-catalysed condensation products",
abstract = "The characterization of phenol-formaldehyde condensates obtained by base catalysis is described. Trimethylsilyl derivatives of the components were prepared and analysed by gas chromatography-mass spectrometry. Electron impact ionization mass spectra of methylolated dihydroxydiphenylmethane positional isomers are discussed. Prominent differences in ion abundances facilitate the identification of the compounds. Substituted trinuclear phenols among the reaction products are also described.",
author = "Laszlo Prokai",
year = "1985",
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AU - Prokai, Laszlo

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AB - The characterization of phenol-formaldehyde condensates obtained by base catalysis is described. Trimethylsilyl derivatives of the components were prepared and analysed by gas chromatography-mass spectrometry. Electron impact ionization mass spectra of methylolated dihydroxydiphenylmethane positional isomers are discussed. Prominent differences in ion abundances facilitate the identification of the compounds. Substituted trinuclear phenols among the reaction products are also described.

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